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Olympus Delta Premium Portable XRF Spectrometer

The Olympus Delta Premium PXRF Spectrometer was purchased in 2014. This is normally a service only instrument, but user training is possible if you contact the lab. The instrument comes with two factory calibrations (Geochem and Soil), as well as calibrations for coal, and can be calibrated to suit a specific sample type.

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PANalytical AXIOS Advanced Simultaneous WDXRF Spectrometer

The PANalytical AXIOS-Advanced WDXRF spectrometer was commissioned in 2010 and is fitted with an SST-MAX X-ray sourcewith a 4kW output and can be operated at 160mA. The resulting high X-ray flux enables high sensitivity and low detection limits for light elements. The AXIOS can measure elements over wide dynamic concentration ranges and include all the elements between Be and U in the periodic table.

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PANalytical MINIPAL 4, EDXRF Spectrometer

The MINIPAL was purchased in 2006. It has a 12 position sample changer and is capble of analysing sodium through to uranium. Data can be optionally processed via full fundamental parameter model and Compton ratio correction, and a standardless program for metal analysis is available.

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PANalytical PW2400 Sequential WDXRF Spectrometer

The PW2400 was purchased in 1996 and has a 102 position sample changer for unattended operation of large batches of samples. The instrument runs SuperQ and Uniquant software and is designed for qualitative, semi-quantitative, and quantitative analysis of a large number of elements, from beryllium to uranium. Trace element levels from 10 ppm to major elements up to 100%.

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PerkinElmer FTIR Spectrometer/Microscope

PerkinElmer FTIR Spectrometer/Microscope

The Spotlight is a Fourier transform infrared (FTIR) spectrometer fitted with with a microscope and attenuated total reflectance (ATR) accessories.

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PerkinElmer Raman Microscope (785 nm)

PerkinElmer Raman Microscope (785 nm)

Raman microscope to enable micron-scale chemical and structural mapping of samples as well as standard point spectra of solids, powders and liquids.

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PerkinElmer UV-Visible Spectrometer

PerkinElmer UV-Visible Spectrometer

The Lambda is a double-beam UV-Visible spectrometer that measures light absorption from the visible to the ultraviolet region (1100 nm to 200 nm, 1.1 eV to 6.2 eV). A sample is usually made up to a known concentration in a non-absorbing solvent (such as water) and loaded into a quartz cuvette (available from the lab). Liquids, solutions and transparent solids can be measured. Note that we are not able to measure reflectance on this instrument.

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Phillips CM200

Phillips CM200

The Philips CM200 field emission transmission electron microscope allows very high resolution images to be obtained from thin (electron transparent) materials. In a field emission gun a very strong electric field is used to extract electrons from a metal filament. This results in an electron beam which is very bright. Ultimately, this microscope allows individual atoms to be imaged. The CM200 TEM allows structural, crystallographic and elemental studies of materials.

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Picoquant Microtime200

Picoquant Microtime200

The Microtime200, manufactured by the German-based PicoQuant GmbH, is generally used in conjunction with the TCS SP5 microscope. By using the lasers from the TCS SP5, the Microtime200 is capable of measuring how fast proteins move within the cell (diffusion) and protein to protein interactions.

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Precision X-ray X-Rad 320 Biological Irradiator

Precision X-ray X-Rad 320 Biological Irradiator

The X-Rad 320 is a self contained biological irradiator for in vivo and in vitro applications.

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Raman

Raman spectroscopy

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Renishaw inVia 2 Raman Microscope (532, 633, 785 nm)

Renishaw inVia 2 Raman Microscope (532, 633, 785 nm)

The inVia 2 is a Raman spectrometer coupled to a microscope. The microscope focuses a laser source onto specific areas of a sample then collects the light scattered off the surface of the sample and directs it through a Raman spectrometer.

Capabilities of the inVia 2 Raman Microscope:

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Renishaw inVia Raman Microscope (325, 442 and 514 nm)

Renishaw inVia Raman Microscope (325, 442 and 514 nm)

The inVia is a Raman spectrometer coupled to a microscope. The microscope focuses a laser source onto specific areas of a sample then collects the light scattered off the surface of the sample and directs it through a Raman spectrometer.

Capabilities of the inVia Raman Microscope:

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SC-XRD Kappa Apex (Bruker) Single Crystal Diffractometer

The Bruker Kappa Apex is fitted with an Incoatec molybdenum X-ray microfocus source to determine the molecular and crystal structure of materials from a single crystal. The instruments is usually operated on a service-basis by an experienced crystallogrpahy, although user training is encouraged.

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Shimadzu HPLC

The Shimadzu Prominence HPLC system is used for both analytical and semi-preparative separations. The instrument is equipped with fluorescence, photo diode array (PDA), and evaporative light scattering (ELSD) detectors, and is combined with a fraction collector. The instrument has a multitude of set-ups and combination and is capable of delivering both isocratic and gradient solvent elution from 0.2 to 10.5 mL/minute.

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Shimadzu UFLCxr

The Shimadzu XR Prominence HPLC system is used for analytical separations. The instrument has a binary pump set-up to allow both isocratic and gradient elution at high back pressures (circa 14 000 Psi), and is equipped with a photo diode array detector (PDA). A wide range of separations are performed on the instrument encompassing both normal and reverse phase conditions, with a wide variety of column chemistries utilised for identification and quantitative analysis.

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Smartlab (Rigaku) 9kW rotating anode thin-film XRD

High intensity (9kW) rotating copper anode X-ray source for rapid analysis of thin films.

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SPEX Freezer/Mill 6970D

SPEX Freezer/Mill 6970D

Milling of solid materials under cryogenic conditions

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Stylus Profiler

The Alpha-Step D-600 provides rapid, high resolution 2D and 3D profiling of a sample surface with a vertical range of 1200 micrometers and sub-Angstrom resolution. The instrument has a high resolution camera for visualising the sample, and a 200 mm motorised stage with a range of motion of 150 x 178 mm. The data is particularly useful for calibrating depth profiles performed on the XPS or TOFSIMS.

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TA Instruments NanoDSC

This capillary Differential Scanning Calorimeter can be used for investigating the stability of proteins, nucleic acids, lipids and other macromolecules. Differential Scanning Calorimetry (DSC) is the only method that directly measures the stability of macromolecules in solution. The information obtained provides valuable insights into the factors (e.g. hydrophobic interactions, hydrogen bonding, conformational entropy and physical environment) that stabilize these biomolecules alone or as complexes, such as protein-ligand or micellar complexes.

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Thermo ESCALAB250Xi X-ray photoelectron spectrometer (XPS)

Thermo ESCALAB250Xi X-ray photoelectron spectrometer (XPS) with depth profile and elemental imaging capability.

- Monatomic argon ion beam for depth profiling

- Helium source for ultraviolet photoelectron spectroscopy (UPS) 

- Variable temperature stage 

- 4-axis variable angle stage for angular-resolved XPS (can improve surface sensitivity)

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Thermo Focus DSQ

The Thermo DSQ II GC-MS instruments are our most up-to-date instruments for analysis of compounds that are sufficiently volatile to enter the gas phase intact. The Focus DSQ II GC-MS instrument at our Lower Campus mass spectrometry facility is configured as an electron impact (EI+) only system and is dedicated to analysis of gaseous environmental samples and for trace level analysis of underivatised volatile organic molecules in solution.

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Thermo LTQ FT

Thermo Scientific LTQ FT Ultra combines the most advanced Ion Trap and Fourier Transform Ion Cyclotron Resonance (ICR) technologies into a single instrument. The ICR cell design produces enhanced sensitivity and greater dynamic range. It is an ultra high resolution instrument for LC/MS with unprecedented analytical power and versatility. The instrument is provided with ESI, nano ESI and APCI ionization sources and CID and ECD fragmentation technologies.

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